7-Sep-2021 News Discovery of Tetrapropylammonium perruthenate

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In the absence of an oxidant, tetrapropylammonium perruthenate (TPAP) is reduced by 2-undecanol to a low-valent ruthenium species that efficiently catalyzes the isomerization of a wide range of allylic alcohols into the corresponding saturated carbonyl derivatives [Eq.(1)]. R1, R2, R3, R4 = alkyl, aryl, H.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Compounds of the formula: wherein R1, Y, W, A and R2 are as defined above are inhibitors of rotamase enzymes in particular FKBP-12 and FKBP-52. The compounds therefore moderate neuronal regeneration and outgrowth and can be used for treating neurological disorders arising from neurodegenerative diseases and nerve damage.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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The reaction rate of a catalyzed reaction is faster than the reaction rate of the uncatalyzed reaction at the same temperature.114615-82-6, Name is Tetrapropylammonium perruthenate, molecular formula is C12H28NO4Ru. In a Patent,once mentioned of 114615-82-6, Recommanded Product: Tetrapropylammonium perruthenate

Disclosed is a synthesis method of chiral tetrahydroquinoline derivatives. According to the present invention, chiral tetrahydroquinoline derivatives having high optical purity can be efficiently synthesized from cinnamyl alcohol derivatives using tetrapropylammonium perruthenate as a catalyst and a chiral catalyst in the presence of oxygen (O_2).COPYRIGHT KIPO 2016

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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The first total synthesis of violaceoid A, a cytotoxic agent, and the asymmetric total synthesis of (-)- and (+)-violaceoid B are reported. The precursor was accessed by desymmetrization of a substituted quinol moiety, and the racemic secondary alcohol was kinetically resolved using a chiral nucleophilic catalyst. The asymmetric synthesis of (-)- and (+)-violaceoid B elucidated the absolute configuration of the naturally occurring violaceoid B. Synthetic violaceoid A inhibited the growth of human breast cancer cell lines MCF-7 and Hs 578T at concentrations of less than 100 muM, while (S)- and (R)-violaceoid B were inactive.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Provided herein are formulations, methods and substituted tetrahydrofuranyl-pyrrolo[1,2-f][1,2,4]triazine-4-amine compounds of Formula (I) for treating Pneumovirinae virus infections, including respiratory syncytial virus infections, as well as methods and intermediates for synthesis of tetrahydrofuranyl-pyrrolo[1,2-f][1,2,4]triazine-4-amine compounds.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Compounds of formula (I): wherein R1, R2 and R3 are defined in the specification. The compounds are useful for treating or reducing the risk of reversible obstructive airways disease

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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This invention describes C1-C6-epothilone fragments and an efficient process for the production of C1-C6-fragments of epothilones and derivatives thereof.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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The present invention relates to phenoxy-azetidine derivatives of Formula I, processes for preparing them, pharmaceutical compositions containing them, and their use as pharmaceuticals as modulators of sphingosine-1-phosphate receptors.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Background: Propargyl compounds such as propargyl alcohols and propargyl amines having several reactive centers have attracted a lot of attention for their various transformation. In particular, these compounds have been recently used as the versatile synthons in the synthesis of various heterocycles via their intramolecular cycloisomerization or cyclocondensation with other unsaturated compounds under different conditions. Conclusion: In this mini-review paper, we focus on summarizing the recent advances in the synthesis of oxygen- and nitrogen-heterocycles by using propargyl alcohols, propargyl amines and their derivatives as one of reactants.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI

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Although there are many methods for oxidizing alcohols on a small laboratory scale, many of these methods are problematic for larger-scale industrial application due to safety and environmental concerns.[1] For example, the use of stoichiometric chromium reagents is very undesirable. In the last 10 to 20 years, there has been a growing momentum in academic efforts to develop catalytic methods for the oxidation of alcohols.[2] There are a now a wide variety of methods that utilize a range of transition metals, enzymes, and organocatalysts as catalysts and employ a number of different terminal oxidants. In this chapter, we will focus on the use of nitroxyl radical based catalysts. Catalytic methods using this class of radicals have evolved in the last 10 years, and they have a number of advantages over many of the alternatives. For example, nitroxyl-based systems have superior substrate scope/functional-group tolerance compared to precious-metal catalysts. In the case of some industrial applications, the avoidance of precious metals is also an advantage from a cost and toxicity point of view.

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Reference:
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI