Synthetic Route of C9H8BNO2. The mechanism of aromatic electrophilic substitution of aromatic heterocycles is consistent with that of benzene. Compound: Quinolin-6-ylboronic acid, is researched, Molecular C9H8BNO2, CAS is 376581-24-7, about Copper-Mediated DNA-Compatible One-Pot Click Reactions of Alkynes with Aryl Borates and TMS-N3. Author is Qu, Yi; Wen, Huanan; Ge, Rui; Xu, Yanfen; Gao, Hong; Shi, Xiaodong; Wang, Jiangong; Cui, Weiren; Su, Wenji; Yang, Hongfang; Kuai, Letian; Satz, Alexander L.; Peng, Xuanjia.
We report a DNA-compatible copper-mediated efficient synthesis of 1,2,3-triazoles via a one-pot reaction of aryl borates with TMS-N3 followed by a click cycloaddition reaction. Employing the binuclear macrocyclic nanocatalyst Cu(II)-β-cyclodextrin, the reactions were performed under mild conditions with high conversions and wide functional group tolerance. We also demonstrate the reaction application toward a one-pot DNA-compatible intramol. macrocyclization. Our optimized reaction protocol results in no significant DNA damage as judged by qPCR anal. and Sanger sequencing data.
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