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The first total synthesis of the title diterpene was accomplished starting from the Wieland?Miescher ketone. A diastereoselective sulfa-Michael addition enabled the generation of the delicate beta,gamma-unsaturated ketone moiety, while the tetracyclic kempane skeleton was readily constructed through domino metathesis.
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Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI