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Optically active transition metal complexes. XCVIII. Synthesis and structure of diastereomers of <(-)-Norphos>Ru(II)(eta5-C5H5)I
Two diastereomers of the <(-)-Norphos>Ru(II) complex with eta5-C5H5 and iodide as ligands were synthesized by a phosphine-exchange reaction between (Ph3P)2Ru(II)(eta5-C5H5)Cl and (2R,3R)-(-)-Norphos, followed by Cl/I displacement.Each of the diastereomers can be separated and their structures and chiroptical properties are discussed on the basis of 1H NMR spectroscopy, circular dichroism, and X-ray crystallography.
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Reference£º
Highly efficient and robust molecular ruthenium catalysts for water oxidation,
Catalysts | Special Issue : Ruthenium Catalysts – MDPI