Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials.50982-12-2, name is Dichloro(cycloocta-1,5-diene)ruthenium(II) A new synthetic method of this compound is introduced below., 50982-12-2
50982-12-2, Toluene (5 ml) was added to a mixture of (Ad2PCH2CH2)2NH (250 mg, 0.37 mmol) and [RuCl2(cod)]n (104 mg, 0.37 mmol) under argon and the mixture refluxed for 20 hours. The mixture was cooled to room temperature and4-methoxyphenyl isonitrile (49 mg, 0.37 mmol) added and the mixture refluxed for 12 hours under argon. It was cooled to room temperature and ether (40 ml) added. The pale brown solid was filtered, washed with ether and dried under vacuum. Yield = 0.18 g.
50982-12-2 is used more and more widely, we look forward to future research findings about Dichloro(cycloocta-1,5-diene)ruthenium(II)
Reference£º
Patent; HADEED, Gerald, S.; ABDUR-RASHID, Kamaluddin; (61 pag.)WO2018/193401; (2018); A1;,
Highly efficient and robust molecular ruthenium catalysts for water oxidation
Catalysts | Special Issue : Ruthenium Catalysts – MDPI