As a common heterocyclic compound, it belongs to ruthenium-catalysts compound, name is Dichlorotris(triphenylphosphino)ruthenium (II), and cas is 15529-49-4, its synthesis route is as follows.
A 50 ml three-necked flask equipped with a stirring reflux device was charged with 1 mmol of 2-diphenylphosphineaniline,1.5 mmol of m-ethoxybenzyl alcohol, 1 mmol of bis (diphenylphosphinoethane), 1 mmol of RuCl2 (PPh3) 3, 1.5 mmol of sodium hydroxide and 20 ml of benzene at a temperature of 100 C for 24 h under a nitrogen atmosphere,After cooling and filtering, the obtained solid was recrystallized from a mixed solvent of CH 2 Cl 2 and petroleum ether to give product 4 in a yield of 86%.
15529-49-4, In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles.,15529-49-4 ,Dichlorotris(triphenylphosphino)ruthenium (II), other downstream synthetic routes, hurry up and to see
Reference£º
Patent; Luoyang Normal College; Li Hongmei; Xu Chen; Zu Enpu; Xiao Zhiqiang; Han Xin; (12 pag.)CN104804048; (2017); B;,
Highly efficient and robust molecular ruthenium catalysts for water oxidation
Catalysts | Special Issue : Ruthenium Catalysts – MDPI