As a common heterocyclic compound, it belongs to ruthenium-catalysts compound, name is Dichlorotris(triphenylphosphino)ruthenium (II), and cas is 15529-49-4, its synthesis route is as follows.,15529-49-4
A 50 ml three-necked flask equipped with a stirring reflux device was charged with 1 mmol of 2-diphenylphosphineaniline,1.1 mmol of p-methylbenzyl alcohol, 1 mmol of 2-diphenylphosphinophenyl ether, 1 mmol of RuCl2 (PPh3) 3, 1.4 mmol of triethylamine and 20 ml of dioxane were added and the mixture was heated at 110 C for 12 h under a nitrogen atmosphere.After cooling and filtering, the resulting solid was recrystallized from a mixed solvent of CH 2 Cl 2 and petroleum ether to give product 14 in a yield of 86%.
With the complex challenges of chemical substances, we look forward to future research findings about 15529-49-4,belong ruthenium-catalysts compound
Reference£º
Patent; Luoyang Normal College; Li Hongmei; Xu Chen; Zu Enpu; Xiao Zhiqiang; Han Xin; (12 pag.)CN104804048; (2017); B;,
Highly efficient and robust molecular ruthenium catalysts for water oxidation
Catalysts | Special Issue : Ruthenium Catalysts – MDPI